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Nanosized ZnNb2O6 photocatalysts (band gaps ~4.0 eV) were successfully synthesized via a citrate complex method. Their particle sizes ranged from 50 to 150 nm. The result of Mott–Schottky measurement revealed that the flat-band potential of ZnNb2O6 was ca. −1.3 V versus Ag/AgCl at pH 6.6. The photocatalytic activities of the samples for the degradation of methyl orange were evaluated under UV-light...
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