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The EPR spectra of high-spin Co(II) systems typically consist of poorly resolved resonances, broadened by a combination of large g-anisotropy, sizable spin–orbit couplings and admixture of excited state character into the magnetic ground state. In this report, we present dual-mode EPR studies of a set of 4-, 5- and 6-coordinate Co(II) complexes, as well as cobalt-substituted carbonic anhydrase, with...
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