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Reported in this paper is a solvothermal synthesis of highly porous polydivinylbenzene. The nanoporous structures of the resultant polymers could be modulated from macro/mesoporosity to meso/microporosity by simply changing the amount of acetone solvent in the synthesis. A micro-phase separation during the solvothermal process was found to be the key factor for this transition in porous structures...
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