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Here, a facile and novel strategy for the preparation of Cu‐doped RuO2 hollow porous polyhedra composed of ultrasmall nanocrystals through one‐step annealing of a Ru‐exchanged Cu‐BTC derivative is reported. Owing to the optimized surface configuration and altered electronic structure, the prepared catalyst displays a remarkable oxygen evolution reaction (OER) performance with low overpotential of...
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