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Palladium-catalyzed alkoxycarbonylation of allyl bromide to unsaturated esters in supercritical carbon dioxide (sc-CO2) was performed and compared with alkoxycarbonylation in organic solvents in this paper. Effects of the catalytic precursor, triphenyl phosphine ligand, base, pressure, and reaction temperature on the reaction yield and selectivity were mainly discussed. The results showed that sc-CO...
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