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The preparation of hydroxyapatite(HAP) in microemulsion media of TritonX-100-n-Pentanol-Cyclohexane- Water have been investigated. The composition and morphological properites of the samples were researched by Fourier-transformed infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), X-ray diffraction (XRD) and adsorption/desorption isotherms of N2 techniques. From the pore size distributions...
A highly sensitive and selective spectrophotometric method is proposed for the determination of trace lead in food. The method is based on the reaction of lead(II) with a new analytical reagent trihydroxyphenylfluorone (TH-PF). TH-PF reacts with lead(II) and form a stable 1 : 2 complex at pH 10.40. Its apparent molar absorption coefficient and Sandell's sensitivity at 580 nm are 4.56 times 104 L/mol/cm...
Experiments indicated that protein can enhance the fluorescence of the 4-chlorosulfo-(2′-hydroxylophenylazo)-rhodanine-Ti(IV) complex [ClSARP-Ti(IV)] in the presence of bis(2-ethylhexyl)sulfosuccinate sodium salt (AOT) microemulsion. Based on this, a sensitive and reproducible fluorometric method for the determination of micro amount protein was developed. The calibration curves of four proteins were...
A novel highly sensitive and selective fluorescent reagent, 2,6,7-trihydroxy-9-(3,5-dibromo-4-hydroxyphenyl)fluorone (DBH-PF) has been studied for the spectrofluorimetic determination of antimony(III) in cetyltrimethylammonium bromide (CTMAB) microemulsion media. DBH-PF reacts with antimony(III) forming a complex with 1:2 (metal to ligand) antimony-DBH-PF in the system of HAc-NaAc buffer solution...
A new method using microemulsified samples is presented. It is for the determination of chromium naphthenate in gasoline by flame absorption spectroscopy. The method has the advantage of simplicity, speed and the use of aqueous standards for calibration instead of organic standards. Coexistent elements do not disturb the determination. Results obtained by this method were better than those obtained...
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