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Advanced multifunctional sponge‐type materials are obtained following chemical treatment of a Visible Light Photocatalyst (VLP) with an alkali aqueous solution under selected conditions. The resulting multifunctional material is fully characterized by XRD, SEM/EDX, TEM, FT‐IR, RAMAN, and UV‐Vis. It is found that the resulting material has high affinity to cationic dyes such as methylene blue (MB)...
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