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Ti 3 SiC 2 powder was milled by high-energy ball milling under argon atmosphere and subsequently thermally annealed. The microstructure evolution of Ti 3 SiC 2 after milling was investigated. It was found that 200nm particle size Ti 3 SiC 2 powder could be achieved by 9h milling whereas a longer milling time would induce Ti 3 SiC 2 decomposition...
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