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Developing highly active and stable nitrogen reduction reaction (NRR) catalysts for NH3 electrosynthesis remains challenging. Herein, an unusual NRR electrocatalyst is reported with a single Zn(I) site supported on hollow porous N‐doped carbon nanofibers (Zn1N–C). The Zn1N–C nanofibers exhibit an outstanding NRR activity with a high NH3 yield rate of ≈16.1 µg NH3 h−1 mgcat−1 at −0.3 V and Faradaic...
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