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An alkynyl‐protected gold nanocluster [Au24(CCPh)14(PPh3)4](SbF6)2 has been prepared by a direct reduction method. Single‐crystal X‐ray diffraction reveals that the molecular structure contains a Au22 core that is made of two Au13‐centered cuboctahedra that share a square face. Two staple‐like PhCCAuCCPh motifs are located around the center of the rod‐like Au22 core. This Au24 nanocluster is...
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