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Spin–orbit charge‐transfer intersystem crossing (SOCT‐ISC) is useful for the preparation of heavy atom‐free triplet photosensitisers (PSs). Herein, a series of perylene‐Bodipy compact electron donor/acceptor dyads showing efficient SOCT‐ISC is prepared. The photophysical properties of the dyads were studied with steady‐state and time‐resolved spectroscopies. Efficient triplet state formation (quantum...
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