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To develop the functional particles with better flame‐retardant and compatibility with epoxy resin (EP) matrix, organic–inorganic double‐shell microencapsulated aluminum hypophosphite (MSiAHP) was prepared by situ polymerization. The water contact angles of MSiAHP (62.4°) is significantly larger than that of aluminum hypophosphite (34.4°), which shows that the organic shell material of MSiAHP endows...