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The formation of complex salt [Ag(PPh3)4][2-B10H9NH3 ∙ 2DMF] (I) by the reaction of the salts of the [2-B10H9NH3]– anion with [Ag(PPh3)4]NO3 is studied. The anionic moiety of complex I is a stable solvate linked by hydrogen bonds of two types. Compound I is identified by IR spectroscopy and elemental, X-ray structure, and X-ray diffraction analyses (CIF file CCDC no. 1884451).
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