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The microstructure of polycrystals is known to govern the performance of structural materials. This drives the need for mechanical characterization methods capable of probing large representative volumes at the grain and sub‐grain scales. In this paper, the use of in situ diffraction contrast tomography (DCT) along with far‐field 3D X‐ray diffraction (ff‐3DXRD) at the Psiché beamline of Soleil is...