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A new microporous metal organic frameworks Eu2(olz)3·7(DMF), based on olsalazine, has been successfully designed and synthesized. Eu‐olz has three‐dimensional structure with dinuclear rare earth cluster and drug molecule olsalazine as ligand, and features as low toxic MOF materials. The Eu‐olz exhibits weak fluorescent emission which can be ascribed to the luminescence of the organic ligand.
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