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Hierarchical lithium iron phosphate/carbon (LiFePO4/C) microspheres were fabricated successfully using a facile spray drying-assisted coprecipitation method. A relatively short calcination time and a relatively low calcination temperature were adopted to prepare the hierarchical LiFePO4/C microspheres. The hierarchical microspheres consisted of nanoparticles with a uniform coating of amorphous carbon...
Nano- and micro-sized LiFePO4 powders were synthesized by a sodium gluconate (C6H11NaO7)-assisted hydrothermal synthesis method at 220°C for 10h with pH=2–7. The resulting powders were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM), and energy-dispersive X-ray spectrometer (EDS). The obtained data showed that the pH of synthesis solution played a key role in the formation...
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