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Mesoporous C-doped TiO2 single crystals with oxygen vacancy (VO-MC TiO2) have been prepared through a facile in-situ modified sol-gel synthesis. The oxygen vacancy of C-doped TiO2 is controlled by the limited-oxygen atmosphere originates from the decomposition of urea. The as-prepared VO-MC TiO2 shows a well-defined cubic morphology with average grain size of 22 nm. The N2 adsorption-desorption isotherms...
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