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We report for the first time the microscopic spacial effect on the dispersion polymerization of methyl methacrylate (MMA) in supercritical carbon dioxide (scCO 2 ). A variety of different-sized high-pressure vessels including microstructured holey optical fiber were employed to conduct the polymerization reactions. The molecular weights of the polymer products indicate that the function of...
This paper describes the development and application of power compensation calorimetry equipment to monitor the dispersion polymerisation of methyl methacrylate in supercritical carbon dioxide. We have studied the polymerisation of methyl methacrylate using a macromonomer (poly(dimethylsiloxane) monomethacrylate) as stabiliser and initiator azoisobutylnitrile. The calorimetric data allow monitoring...
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