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In this study, we propose F2‐selective 2D NMR spectroscopy as an effective method to obtain high‐quality spectra of minor components in complex foodstuffs. Selective excitation along the F2 axis overcame the problems occurring in the conventional F1‐selective 2D NMR spectroscopy. The technique was successfully applied to mango juice to provide high‐quality TOCSY, DQF‐COSY, and NOESY spectra of the...
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