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In situ Raman spectroscopy has been used to investigate the mechanism of dimethyl carbonate (DMC) synthesis via the reaction of methanol with carbon dioxide over zirconia. Methanol adsorption leads to the appearance of adsorbed methoxide groups, whereas CO2 adsorption leads to the formation of carbonate species. Monomethyl carbonate species, (CH3O)COO(Zr)2, are formed by the reaction of methoxide...
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