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Herein, inspired by the specific detection of the commercial dithizone to Zn2+, a series of polyacylhydrazones (PAHZs) with polymerization‐induced emission (PIE) properties are successfully prepared and applied to the specific recognition and detection of Zn2+. It is found that all selected monomers do not emit fluorescence. In contrast, the as‐prepared PAHZs can emit strong fluorescence at 455 nm,...