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In order to enhance ultra-thin palladium (Pd) membranes integrity, an improved photocatalytic deposition method (PCD) was developed for the Pd/TiO 2 composite membranes. The PCD reactions for Pd membranes occurred in the solution previously and the mechanism of the improved PCD method is interpreted by the photocatalytic reaction at the TiO 2 semiconductor/Pd(II) liquid film interface...
Ultra-thin palladium membranes (0.2 μm thickness) on TiO 2 supports were obtained by photocatalytic deposition. The presence of EDTA in an aqueous precursor solution for the Pd membranes was found to promote the formation of Pd membranes; the effect of chelating agents deposited on the Pd membrane was analyzed by SEM, EDS, and XPS. Compared with previous work in our laboratory, the photocatalytic...
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