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Cancer recurrence and metastasis are two major challenges in the current clinical therapy. In this work, a novel diketopyrrolopyrrole‐based photothermal reagent (DCN) with unique J‐aggregation‐induced redshift is synthesized to achieve efficient tumor thermal ablation under safe power (0.33 W cm−2). Meanwhile, S‐nitroso‐N‐acetylpenicillamine (SNAP) is co‐loaded with near‐infrared‐absorbing DCN in...