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The first two amino-substituted BEDT-TTF derivatives, aminomethyl-ET (AMET) and aminoethyl-ET (AEET), have been prepared; the critical step in both cases was a hetero Diels-Alder reaction with 1,3-dithiole-2,4,5-trithione. AEET shows expected reactivity towards electrophiles whereas AMET will not react with aryl acid chlorides or sulfonyl chlorides, but amides of AMET can be produced by DCC coupling...
The syntheses of eight derivatives of BEDT-TTF (ET) containing pyridine, 2,2′-bipyridine or 2,4′-pyridylpyrimidine binding sites on a side chain are reported, for use in the preparation of organic/inorganic hybrid materials. The intermediate hydroxyethyl derivative of BEDT-TTF is prepared in an efficient five-step procedure.
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