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LiMn1.5Ni0.5O4 cathode materials for lithium ion batteries (LIBs) were synthesized by the low cost wet-chemical Pechini technique. Phase analysis by X-ray diffraction shows that extended heat treatment at 900°C causes precipitation of LixNi1−xO with consequent reduction in specific energy capacity. Raman spectroscopy and powder neutron diffraction have been extensively integrated into characterization...
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