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The intermetallic zinc compounds AAu4Zn2 (A = Ca, Ce, Pr, Nd) were obtained by induction melting of the elements in sealed tantalum tubes. The samples were studied by X‐ray diffraction on powders. The structures of the calcium and the cerium compound were refined from single crystal diffraction data: YbAl4Mo2 type, I4/mmm, a = 692.8(1), c = 527.6(1) pm, wR2 = 0.0304, 244 F2 values and 11 variables...
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