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Zr 5 Ni 4 Al was synthesized by arc-melting of the elements and subsequent annealing in an induction furnace at 1360–1440K. This aluminide crystallizes according to X-ray diffraction data of a twinned crystal with an ordered version of the Zr 3 Al 2 type: P4 2 /m, a=716.7(3), c=659.8(4) pm, wR2=0.1174, 824 F02 values, 28 variables. Due to the ordering of the...
The intermetallic compounds IrIn2-xMgx (x=0.53, 0.70) and Mg3-xInxIr (x=0.80, 0.97) were synthesized by induction melting of the elements in glassy carbon crucibles in a water-cooled sample chamber. All compounds were investigated by X-ray powder diffraction and the structures have been refined on the basis of single-crystal diffractometer data: Mg2Cu type, Fddd, a=981.9(3), b=528.8(1), c=1799.2(4)...
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