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A novel mesoporous ZrO 2 immobilized magnetic Fe 3 O 4 microsphere (m-ZrO 2 @Fe 3 O 4 ) was successfully synthesized and characterized by transmission electron microscope (TEM), X-ray diffractometer (XRD), nitrogen adsorption measurement (NAM), energy-dispersive X-ray analysis (EDX), vibrating sample magnetometer (VSM). Then the resultant m-ZrO 2...
The electrochemical characteristics of a novel all diamond fabricated boron-doped diamond microelectrode array (BDD-MEA) are critically appraised. The voltammetric response of simple electron transfer processes has been investigated and found to generate sigmoidal voltammetric curves. Furthermore, the device has been utilized for various analytical applications including, the direct detection of 4-nitrophenol...
The electrochemical behaviour and cation recognition properties of two oxaferrocene cryptand ligands, 1,1′-[(1,4,10-trioxa-7,13-diazacyclopentadecane-7,13-diyl)diethoxy]-3,3′,4,4′-tetraphenylferrocene and 1,1′-[(1,4,10,13-tetraoxa-7,16-diazacyclooctadecane-7,16-diyl)diethoxy]-3,3′,4,4′-tetraphenylferrocene, have been characterized in acetonitrile in the presence of Ba 2+ and Na + by...
In this report, we derivatise carbon powder with anthracene, azobenzene, diphenylamine, 9,10-diphenylanthracene, methylene blue, 3-nitrofluoranthene, 6-nitrochrysene, 9-nitroanthracene, 9,10-phenanthraquinone (PAQ), thionin, and fast black K (2,5-dimethoxy-4-[(4-nitrophenyl)azo]benzenediazonium chloride) and separately immobilise the resulting material onto a bppg electrode. We use cyclic voltammetry...
The determination of sulphide at an electrochemically generated nickel oxide layer at glassy carbon and screen-printed electrodes in acidic media has been examined and appraised. The NiO layer was found to produce a stripping-like signal to sulphide and gave a linear peak current response from 20 to 90 μM. The response was further enhanced by repetitive cycling allowing accumulation of nickel sulphide...
A simple pH probe is developed based upon the covalent chemical derivatisation of carbon particles with anthraquinone. The amperometric response of electrodes constructed from this material is examined and shown to produce a Nernstian linear response to pH from 1 to 9, over a range of temperatures from 20 to 70 o C, consistent with a two-electron, two-proton electrochemical process.
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