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A new self-assembly protocol leading to the formation of heteronuclear coordination cage 10 is reported. Reaction of tetradentate cavitand ligand 1, bearing one ethynylpyridine and three benzonitriles at the apical positions, with Pt(dppp)OTf 2 and Pd(dppp)OTf 2 in a 1:3 ratio yields 10 as the thermodynamic product. Under the same conditions, the self-assembly of 1 with either Pt or...
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