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Surface-enhanced Raman spectroscopy (SERS) has been utilized as an in-situ probe of adsorbed species and surface reaction intermediates during the reduction of nitric oxide by either carbon monoxide or hydrogen over polycrystalline Rh films. SERS-active Rh surfaces were prepared by electrodeposition of ultrathin films on electrochemically roughened gold and display remarkably robust SERS activity...
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