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An efficient synthesis of 4β-aminopodophyllotoxin from 4β-bromopodophyllotoxin using ammonia, and also a facile synthesis of 4β-amino-4'-O-demethylpodophyllotoxin from 4β-azidopodophyllotoxin by simultaneous azido reduction and selective demethylation at 4'-position employing chlorotrimethylsilane and sodium iodide, has been described. These are potential precursors for the various 4β-amino analogs...
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