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Using ammonium dodecyl sulfate (ADS) as the surfactant, the response of three common interfaces in the direct coupling of microchip micellar electrokinetic chromatography with electrospray ionization mass spectrometry was studied. In the range of 10–40 mM surfactant, a conventional sheath liquid interface provided poorer sensitivity than both sheathless interface and low‐sheath‐flow interface. At...
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