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The origin of a two-stage endothermic reaction in Zr36Ti24Be40 metallic glass was investigated by differential scanning calorimetry (DSC), thermo-mechanical analyzer (TMA) and high resolution transmission electron microscopy (HREM). HREM image of a specimen heated to 420°C under a constant applied tensile stress of 3 MPa showed the formation of medium-range-ordered clusters 1 nm to 2 nm in size. This...
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