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Pervaporation has great potential in the separation of many significant mixtures. However, excessive penetration of separation layer into the substrate pores enhances the transport resistance of solvent molecules, which impedes the development of pervaporation membrane. In this study, a facile floating‐on‐water (FOW) method was used to prepare poly(dimethylsiloxane) (PDMS)/polytetrafluoroethylene...
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