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The crystal structures of complex zirconium fluorides (C2H5N4)2Zr2F10·H2O and (H3O)3(NEt4)2Zr4F21·3H2O synthesized for the first time are determined. The formation of new structure types of polymeric chain complex anions is found in them. Two crystallographically independent zigzag-like polymeric chains ∞(ZrF5)− composed of pentagonal bipyramidal polyhedra of Zr atoms sharing F-F edges form a polymeric...
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