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Linear, α‐branched, and β‐branched aliphatic amines are widespread in pharmaceuticals, agrochemicals, and fine chemicals. Thus, the development of direct and efficient methods to these structures in a tunable manner is highly desirable yet challenging. Herein, a catalyst‐controlled synthesis of α‐branched, β‐branched and linear aliphatic amines from Ni/Co‐catalyzed regio‐ and site‐selective hydroalkylations...
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