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Four binuclear cadmium(II) cryptates have been synthesized by [2 + 3] Schiff-base condensation of tris(3-aminopropyl)amine with sodium 2,6-diformyl-4-R-phenolates (R = OCH 3 , CH 3 , Br and Cl) in the presence of Cd(ClO 4 ) 2 6H 2 O. The crystal structure of the cryptate of macrocyclic L 3 (R = Br) [CdL 3 ](ClO 4 ) was determined by...
A new binuclear cadmium(II) macrocyclic complex has been synthesized by [2 + 2] Schiff-base condensation of tris(3-aminopropyl)amine with sodium 2,6-diformyl-4-methoxylphenolate in the presence of Cd(ClO 4 ) 2 6H 2 O. The crystal structure, spectral characterization and molar conductivity show that two cadmium(II) ions were bridged by two μ 2 -phenoxy oxygen atoms....
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