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Organic–inorganic hybrid materials suitable for the development of sol–gel coatings for metallic surfaces were prepared by hydrolysis and condensation of γ-methacryloxypropyltrimethoxysilane (MAPTMS) and tetramethyl orthosilicate (TMOS). The hydrolysis of MAPTMS/TMOS was carried out in an ethanol/water solution. The prehydrolysis stage of MAPTMS/TMOS system was monitored by Fourier transform infrared...