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Novel porous PVDF microspheres have been prepared by a facile electrospraying approach. The microspheres with an average size of 2–5µm in diameter possess inter-connective pores. Several key factors including polymer diffusion, solvent evaporation, chain entanglements and Coulomb fission influence the morphology of final products obtained by electrospraying. About 66wt% sulfur content could be loaded...
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