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A new method for the iodine‐catalyzed reduction of phosphine oxides with phosphites at room temperature is reported. The mild reaction conditions, scalability, and simple purification requirements render it a method of choice for the large‐scale production and facile regeneration of a variety of phosphines. Mechanistic studies, supported by DFT calculations of the oxygen transfer between the starting...
Im Jahr 1669 entdeckte Henning Brand das Element Phosphor, indem er in Urin enthaltenes Phosphat unter harschen Reaktionsbedingungen reduzierte. Das Experiment markiert den Beginn der Phosphorchemie, wobei Brand nicht wusste, dass er P=O‐Bindungen reduziert hatte. P. Li, P. Métivier und R. Wischert beschreiben in der Zuschrift auf S. 16205 eine effiziente, milde und kostengünstige Methode für die...
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