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An Ru‐doping strategy is reported to substantially improve both hydrogen evolution reaction (HER) and oxygen evolution reaction (OER) electrocatalytic activity of Ni/Fe‐based metal–organic framework (MOF) for overall water splitting. As‐synthesized Ru‐doped Ni/Fe MIL‐53 MOF nanosheets grown on nickel foam (MIL‐53(Ru‐NiFe)@NF) afford HER and OER current density of 50 mA cm−2 at an overpotential of...
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