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Tripodal donor‐acceptor (D‐A) small molecules Tr‐Np3 and Tr‐T‐Np3 consisting of triphenyl triazine and 1,8‐naphthalimide, without and with a thiophene spacer have been synthesized. Their optical and redox properties were thoroughly investigated along with their utilization as photocatalysts in organic transformations. Compounds Tr‐Np3 and Tr‐T‐Np3 showed broad absorption in the range of 290–480 nm...