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In this study, an extraction and preconcentration technique using solid‐phase extraction (SPE) along with hollow fiber (HF) has been developed as an ultra‐preconcentration technique for some triazole pesticides in aqueous samples. Triazole pesticides were employed as model compounds to assess the method and were monitored by gas chromatography–flame ionization detection (GC‐FID). Initially, an aqueous...
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