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The addition of bis(pinacolato)diboron [(Me 4 C 2 O 2 )B-B(O 2 C 2 Me 4 )] to α,β-unsaturated carbonyl compounds giving β-boryl carbonyl compounds and the addition to terminal alkynes yielding either 2-boryl-1-alkenes or 1-boryl-1-alkenes were carried out in DMF at room temperature in the presence of CuCl and AcOK. The transmetalation between diboron...
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