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Total ion yield spectrum of perfluorocyclobutane (c‐C4F8) has been measured in the C and F K‐shell excitation regions. The peak assignments are presented based on angle‐resolved photofragment ion mass spectrometry. The peaks at 291.34 and 688.5 eV are found to come from the transitions from the C 1s and the F 1s to the lowest unoccupied b2σCF* orbital, respectively. A photoelectron–photoion–photoion...
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