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Three-dimensional (3D) micrometer-scale spherical titanate nanotube assemblies have been successfully synthesized via hydrothermal synthesis from Ti powders. The obtained titanate nanotube assemblies have a diameter of around 4–7µm. The titanate nanotubes have an outer diameter of around 9–10nm, an inner diameter around 3–4nm and a length of several micrometers. A proposed two-stage growth mechanism...
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