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To advance CaO‐based CO2 sorbents it is crucial to understand how their structural parameters control the cyclic CO2 uptake. Here, CaO‐based sorbents with varying ratios of Na2CO3:CaCO3 are synthesized via mechanochemical activation of a mixture of Na2CO3 and CaCO3 to investigate the effect of sodium species on the structure, morphology, carbonation rate and cyclic CO2 uptake of the CO2 sorbents....
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