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Se- and Te/Se-doped n-type CoSb3 skutterudites were synthesized by high-pressure synthesis (HPS) followed by spark plasma sintering. Se and Te substitutions on the Sb sites were verified by X-ray powder diffraction, energy dispersive spectrometry, and Raman spectroscopy. The experimental determined solubility of Se in CoSb3, was significantly enhanced by HPS technique, and reached a large value of...
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