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Based on difluoroboron β‐diketonates, four novel alanine dipeptides C10H21CO‐Ala‐Ala‐O‐Br‐BF2DPh (4) with long alkyl chains were prepared and characterized. UV and emission in different solvents and in the solid states are studied. The self‐assembly behaviors are investigated by FE‐SEM, CD, and FTIR spectra, and different stereochemical structures are proposed. Hydrogen bonding, π–π interactions,...
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