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Chlorodibenzoxaphosphinine 1Cl reacted with bulky R1Li reagents to give organodibenzoxaphosphinines, which reacted with less bulky R2Li reagents to yield 2‐oxybiphenylylphosphanes. Protection of the air‐sensitive hydroxybiphenylylphosphanes with borane reduced their reactivity. X‐ray analysis gave evidence of intermolecular hydrogen–hydrogen bonds between protic hydroxy and hydridic borane groups...
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